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Materials Science in Additive Manufacturing                           AM-produced CoCrFeMnNi properties




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            Figure 2. Selective laser melting (SLM)-produced CoCrFeMnNi tensile samples. (A) Selected tensile samples attached to the build plate after SLM;
            (B)  dimensions of tensile samples.


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            Figure 3. Charpy test of selective laser melting-produced CoCrFeMnNi. (A) Schematic orientation of Charpy specimen during the test (ASTM E23); (B)  a
            Charpy specimen before and after test.

            equipped with Cu target. The scan was performed in the   usually cause lack of fusion (LOF) defects as laser fails to
            2θ range of 35° to 100° and with tube voltage and current   provide sufficient energy to generate full melting of powder
            of 40 kV and 44 mA, respectively. The fracture surfaces   layers, which leads to the formation of pockets of unmelted
            of Charpy V-notched samples were also characterized   powder particles or even delamination from the previously
                                                                            [44]
            by surface appearance as seen in the scanning electron   deposited layers . The second region of energy density
            microscopy (SEM) images.                           domain is the target for process parameter optimization
                                                               and can be characterized by the reduced porosity fraction.
            3. Results and discussion                          In the third region, excessive overheating caused by high
                                                               energy density generates surface temperatures that exceed
            3.1. Effect of scanning speed on relative density and   the evaporation point of an alloy causing particles and
            porosity                                           molten material to eject from heat-affected zone, resulting
                                                                                 [45]
            The criterion for selecting the proper scanning speed was   in large spherical pores . Strong vaporization and spatter
            based on the porosity or the density of the SLM-produced   lead to shortage of molten metal to fill the molten track.
                                                                                                           [46]
            materials.  Figure 4A shows the optical micrographs of   As  a result,  a printed  part  is left  with  many voids .
            the cross sections of cubic samples obtained under the   Moreover, high energy density may cause vaporization of
            seven scanning speeds. It is clear that the density and size   low melting elements, which becomes entrapped and leads
            of pores increase as the scanning speed decreases. This   to the formation of pores. Inert gas dissolved in the molten
            phenomenon can be explained by the following. It is well   metal and released during solidification as well as moisture
            known that incorrect choices of laser energy density in SLM   present on the surface of powder particles may also be the
                                                                                    [45]
            often result in formation of defects. Depending on defect   source of gaseous porosity .
            types, the energy density domain for SLM can be split   In the present study, energy density optimization was
            into three regions. Low energy densities in the first region   performed by varying the scanning speed, and the scope


            Volume 2 Issue 1 (2023)                         5                        https://doi.org/10.36922/msam.42
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