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Materials Science in Additive Manufacturing                Y O  influence in heat-treated LPBF IN718 composite
                                                                        2  3

            in comparable or better mechanical properties than those   calculated by dividing the length of the line by its number
            reported by other literature as shown in our previous study   of intersections. The diameter of the grain would then be
            Luu et al. .                                       equal to the diameter of the circle that has the same area as
                   [22]
              The grain size was calculated using the line intersection   the width × length.
            method. The width and length of the grains would then be   The size distributions of the precipitates were measured
                                                               using the ImageJ software. Multiple SEM images were
            A                      B                           taken and the size of the precipitates in the images was
                                                               measured. The volume fraction, f , of the precipitates in the
                                                                                         p
                                                               samples was measured using Equation I.
                                                                           4   d  3
                                                                                p
                                                                           3      2      N p        (I)
                                                                       f     Ad
                                                                       p
                                                                                 p
                                                                 Where d  is the mean diameter of the precipitates, N  is
                                                                                                           p
                                                                        p
                                                               the number of precipitates in a given area, and A is the area
                                                               of the given area.
            C                      D
                                                               3. Results and discussion
                                                               3.1. Microstructures of as-printed samples
                                                               SEM images comparing the microstructures of as-printed
                                                               samples are shown in Figure 5A and B. The microstructures
                                                               of both samples consist of a white color phase with a


                                                               Table 4. Labeling of IN718 and the composite samples
                     E
                                                               Sample ID    Heat treatment        Reinforcement
                                                               AP-0        As-printed             Nil
                                                               AP-Y                               Y O 3
                                                                                                   2
                                                               1075-0      Solutionized at 1075°C  Nil
                                                               1075-Y                             Y O
                                                                                                   2  3
                                                               1075A-0     Solutionized at 1075°C+Aged  Nil
                                                               1075A-Y                            Y O
                                                                                                   2  3
            Figure  2. Photos of the powder mixture after 2(A), 4(B), 6(C), and   1275A-0  Solutionized at 1275°C+Aged  Nil
            8(D) hours of mixing. SEM image of the powder mixture after 8 h of    1275A-Y         Y O
            mixing (E).                                                                            2  3


                         A                                     B

















                                             Figure 3. Solutionizing (A) and aging (B) profiles.


            Volume 1 Issue 4 (2022)                         4                      https://doi.org/10.18063/msam.v1i4.25
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