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Materials Science in Additive Manufacturing                   MEX optimization printing of rHPDE from milk jugs



            for manual cutting. Initial attempts to extrude the filament   used in the preliminary tests, which were found to have
            were unsuccessful due to the excessive moisture absorbed   impurities that could have affected the printing outcomes.
            by the flakes from over-handling, thus affecting the melting   For the smooth print surface (Table 2), only two
            consistency in the heating chamber. It is important to keep   permutations of settings successfully produced parts that
            the flakes as dry as possible before feeding them into the   meet the desired conditions. These conditions require
            hopper to ensure a smooth, consistent flow. Throughout   (i) the first print layer to adhere to the print bed during
            the process, the Airpath was maintained at 39% of its   printing and (ii) the part to be easily removed from the
            maximum fan speed, and the temperature directly above   print surface after printing (preferably by hand). For the
            the Airpath was maintained at 21.8°C.
                                                               roughened print surface (Table 3), seven permutations of
            3.2. Optimization of MEX print parameters for      settings were found to meet both these desired conditions.
            rHDPE
                                                               3.2.4. Printing with different print beds and PTs
            The  findings  from  the  four  tests  conducted  on  various
            types of print bed materials, PS, print quality on surfaces   During these tests, a total of 16 permutations of PT and PBT
            with different degrees of roughness, and variations in PBTs   settings were explored. Out of these 16, 11 tests resulted
            and PTs are described in the following sections.   in  print  bed  adhesion  failure.  The  remaining  five  tests
                                                               reported part failure, which indicated that the adhesion
            3.2.1. Printing on different print bed materials   strength was greater than that of the part and thus was not

            From testing on various surfaces, such as the PEI board,   further examined. The peak shear load and failure area for
            vHDPE sheet, hot-pressed rHDPE sheet, masking tape   these prints were recorded (Tables 4 and 5, respectively).
            backing on the PEI board, double-sided tape on PEI   The  resultant  shear strength  of the  print bed  adhesion
            board, ABS board, and the paper side of the foam core,   was then calculated using Equation I and summarized in
            it was observed that print detachment from print bed   Table 6.
            occurred on all these surfaces after printing different   4. Discussion
            number of layers, except for the prints on the rHDPE and
            vHDPE surfaces, where complete prints were achieved   4.1. Recycling milk jugs into rHDPE filaments
            (Table 1).                                         After several attempts to extrude the filament using the
            3.2.2. Printing at various speeds                  different flake sizes, it was observed that it is important to
                                                               maintain the spooling speed slightly faster or at a similar
            A single layer of the model was printed at PS of 5, 15, and   speed to  the  extrusion rate to  achieve  constant  filament
            50 mm/s, with varying degrees of success. It was observed   diameters. However, inconsistencies in the feed material
            that the printed path of materials began to break while   can lead to erratic extrusion rates, highlighting the need to
            printing the first layer at 50 mm/s. There was no breaking   preprocess the flakes to an appropriate size before feeding
            of filament while printing the first layer at 15 mm/s, but   them  in  the  hopper.  Furthermore,  keeping  the  hopper
            the filament was sliding on the print bed during the print   constantly filled during operation ensures a consistent
            as the filament did not adhere sufficiently to the surface of   material feed into the extruder and maintains a steady
            the hot-pressed rHDPE sheet. At 5 mm/s, the sliding was   extrusion rate.
            reduced, but the print detached from the print bed soon
            after being printed.                                 When working with HDPE flakes, it is important
                                                               to prevent moisture from coming into contact with the
              According to Sun  et  al.,  the temperature profile of   surface. Excessive handling or touching the flakes with
                                   17
            the print significantly affects bond formation and print   bare  hands can introduce  unwanted  moisture,  adversely
            bed adhesion. In a test where parts were printed at PS   affecting melting consistency and extrusion rate. It is best
            of 5 mm/s and PBT of 24 (room temperature) and 40°C,   to keep the flakes as dry as possible while filling the hopper,
            the prints at PBT of 24°C did not adhere well to the print   and it is recommended to thoroughly dehydrate the flakes
            bed, while complete prints were achieved with sufficient
            adherence at PBT of 40°C.                          in the oven just before placing them into the hopper.
                                                                 Using  smaller  flake  sizes  provides  better  consistency
            3.2.3. Printing on print bed with different surface   in terms of extrusion rate and filament diameter. Flakes
            roughness                                          larger than 6 mm cause more “popping” or expulsion from
            A  4  mm  vHDPE sheet  was  placed  over  the  PEI  surface   the feeder and obstruction within the hopper, resulting
            of the print bed to ensure better reliability of the results   in a less smooth material feed and flow into the heating
            compared to those of the hot-pressed rHDPE sheets   chamber. In all subsequent tests, the selected flake size for


            Volume 3 Issue 3 (2024)                         5                              doi: 10.36922/msam.4084
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