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International Journal of Bioprinting                                Continuous gradient TPMS bone scaffold






































                                    Figure 3. Three-dimensional model of continuous gradient porous structure.
            follows: G_I (ω = 2), G_II (ω = 3), G_III (ω = 4), P_I (ω = 2),    The morphology and manufacturing defects of the
            P_II (ω = 3), and P_III (ω = 4). The thickness of the models   samples were observed by means of scanning electron
            is set to 0.4 mm. Figure 3 displays the 3D diagrams of the   microscopy (SEM; Model FEI200, FEI, USA).
            two sets of models and their specific parameters.
                                                               2.2.2. Mechanical properties test
               The designed models were manufactured using a   Static  compression  tests  were  conducted  on  a  universal
            metal 3D printing device (L-PBF system CR-PBFM250)   testing machine (MTS 809, MTS Systems Corporation,
            with Ti-6Al-4V material having a particle size of 15–45   Minnesota, USA) equipped with a 10 kN gravity sensor.
            μm. The printing parameters were optimized prior to   The loading rate used was 0.5 mm/min. The elastic
            printing to ensure high-quality products. The laser power   modulus of each sample was calculated from the slope of
            used  was  290  W,  with  a  laser  spot  diameter  of  85  μm.   the linear phase observed at the beginning of each curve.
            The scanning speed was set at 2000 mm/s, and the layer
            thickness was 40 μm. The printing process was carried   2.3. Finite element analysis of continuous gradient
            out under argon protection at a temperature of 26°C   TPMS structure
            to prevent oxidation. Two samples were made for each   2.3.1. Finite element analysis of mechanical properties
            model, and the resulting samples were cleaned using   To establish the initial model, Grasshopper was employed,
            compressed air and ultrasound.                     and the generated STL file was imported into HyperMesh
                                                               software for topology processing in order to regenerate a
            2.2. TPMS structure performance test               refined  mesh.  The  mesh  model  was then  imported  into
            2.2.1. Porosity test                               ABAQUS software. The bottom of the Z-axis was fixed, and
            The total porosity of the samples was determined using the   a 40% strain was applied to the upper part of the Z-axis.
            dry weighing method, and the calculation formula used   The elastic modulus was set to 110 GPa and the Poisson’s
            was as follows :                                   ratio to 0.34. After the simulation, the stress distribution of
                       36
                                                               the TPMS structure was visualized.
                        Porosity   (1  m /  t   V )  (VIII)
                                      s
                                            d
                                                               2.3.2. Finite element simulation of permeability
               where m  is the mass of each sample; ρ  is the theoretical   Six  models  with  varying  porosity  were  selected  for
                     s
                                            t
            density of Ti-6Al-4V (4.42 g/cm ); and V  is the volume set   the study. These models underwent pretreatment in
                                     3
                                            d
            for printing.                                      HyperMesh software before being imported into COMSOL
            Volume 10 Issue 2 (2024)                       316                                doi: 10.36922/ijb.2306
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