Page 228 - IJB-10-5
P. 228

International Journal of Bioprinting                                        Effect of ingredient flow speed




            2.5. Measurement of filament width and actual         where the power law index (n) and flow consistency
            printing speed                                     index (K) are displayed as the function of non-Newtonian
            Measurements of the length and line width of the printed   viscosity (v). The power law index (n) indicates the flow
            straight line were performed thrice using ImageJ software   behavior. A shear-thinning fluid would have  n < 1. A
            (National Institutes of Health, USA). Premium Rush   smaller  n indicates stronger  shear thinning capability of
            (Adobe Inc., USA) was used to locate the two frames when   the fluid. Fluids with small n and K form ideal food inks as
            extrusion occurred, and the time taken for each print   these fluids can be ejected out of the extruder with ease. 50,51
            was measured. The actual printing speed was acquired by   Equation (I) was subsequently linearized into log form to
            dividing the average length of the printed straight line by   determine the value of the power law and flow consistency
            the average time taken for each print.             index (Figure 1B and Equation [II]).

            3. Results                                                   log v = log K + (n – 1) log γ      II
                                                                                              ·
            3.1. Rheological characterization of MP food ink
            To understand the rheological behavior of the MP food   Through curve fitting, the power law index and flow
            inks, viscosity experiments were conducted. The rheology   consistency index are determined to be 0.347 and 131.5,
            results are depicted in Figure 1A, where it can be observed   respectively. These values could be useful for designing
            that the viscosity of the MP food inks decreased at a   any mathematical model.
            high shear rate and increased at a low shear rate. The
            ability to exhibit shear thinning behavior meant that   3.2. 3D printing using dot extrusion
            MP inks are pseudoplastic materials, which is essential
            for food extrusion printing 44,45  as the food has to behave   3.2.1. Effect of nozzle geometry on food extrusion
            like a liquid to be extruded and a solid to form stable   The nozzle is a crucial part of 3D printing as the materials
            self-supporting structures. 46                     would  be  extruded  through this  small orifice. In  3DFP,
                                                               the nozzle diameter is essential to get a robust model.
               The data from the rheological study were then fitted   According to existing 3DFP experiments,  a high-
                                                                                                    45
            to  a  viscosity  model.  According  to  researchers  in  the   resolution 3D model would require a small-sized nozzle
            3DFP field, 40,47  the power law model is a better fit for MP   diameter. However, utilizing a smaller-sized nozzle would
            food  inks  as  compared  to  other  models.   Furthermore,   increase the printing time of the 3D models as compared
                                              48
            the  power  law  model  is  best  suited  for  shear-thinning   to using a larger-sized nozzle. Therefore, the nozzle size
            fluids  and chosen due to the best fit of R  = 0.9991. The   was examined to understand its effect on food extrusion.
                49
                                              2
            relationship between kinematic viscosity (v) and shear rate   With a digital microscope, it was observed that the exterior
             ·
            (γ) was analyzed using Equation (I):               design of the different-sized nozzles was tapered. Even
                                                               though the nozzles were tapered internally, the nozzles
                            v = Kγ                        I    differed  in  terms  of  the  geometry  at  the  orifice.  From
                                · n-1
                                                               Figure 2A, the digital microscope revealed a flat, thin wall






















            Figure 1. Rheological characterization of mashed potato (MP) food ink: (A) viscosity of the MP ink versus shear rate curve, and (B) linearized viscosity
            versus shear rate curve in logarithm form for curve fitting.


            Volume 10 Issue 5 (2024)                       220                                doi: 10.36922/ijb.2787
   223   224   225   226   227   228   229   230   231   232   233