Page 109 - IJB-8-3
P. 109

Yang, et al.

                         A
                                                           D












                         B












                         C














           Figure 4. Optical microstructure of laser-processed parts and the corresponding XRD patterns. (A) Mg. (B) Mg-Sc. (C) mMg-Sc. (D) XRD
           patterns.

           for mMg-Sc specimen, a single-phase microstructure   A                      B
           was  formed.  The  corresponding  XRD  patterns,  as
           depicted in Figure 4D, also revealed the same results.
           In fact, SLM is a rapid prototyping technology using
           high-energy laser beam as processing heat source
           and has great potential in the preparation of non-
           equilibrium alloy. It was believed that the laser has the   C               D
           characteristics of high-energy density and small action
           area. Laser radiation on the non-equilibrium alloy
           powder can make the powder skip the crystallization
           area and melt at a very high heating rate, and then,
           the micro-molten pool is cooled rapidly through
           non-interface heat conduction, which is much higher
           than the critical cooling rate required to form the
           non-equilibrium alloy [42,43] .  Thus, the deposited   Figure 5. The electrochemical test results of samples. (A) OCP
           layer of non-equilibrium alloy structure is obtained.   curves. (B) Polarization  curves. (C) Nyquist plots. (D) |Z|-
           More importantly, SLM can obtain parts through the   frequency plots and phase angle frequency plots.
           superposition of deposition layers [44,45] . A  number of
           studies have proven that SLM process is effective in   MA and then processed by SLM. Results showed that
           preserving the metastable phase. For instance, Hugo   metastable Al Fe  parts were successfully obtained at
                                                                           5
                                                                              2
           et al. [46]   produced  fine  metastable Al-Fe  powders  by   suitable laser processing parameters.
                                       International Journal of Bioprinting (2022)–Volume 8, Issue 3       101
   104   105   106   107   108   109   110   111   112   113   114