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Shuai, et al.
                         A                 B                 C                 D










                         E                 F                 G                 H










                         I                                  J                  K











           Figure 2. Low- and high-magnification SEM images of (A,E) Fe/0.3Mg Si, (B,F) Fe/0.6Mg Si, (C,G)
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           Fe/0.9Mg Si, and (D,H) Fe/1.2 Mg Si composites and corresponding EDS analysis of (I) point A-D and
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                    2
           (J,K) area E.
           contact angle is, the better the hydrophilicity will   refined  with  an  average  grain  size  of  18.6  ±
           be.  This indicated  that  Fe/Mg Si had stronger    1.2 μm. The grains of Fe/1.2Mg Si also exhibited
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           hydrophilicity than Fe. It is considered that high   a smaller size (average grain size of 21.1 ± 1.8 μm)
           hydrophilicity is of significance for bone implants,   in comparison with Fe/0.3Mg Si. However, the
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           which contributes  to corrosion attack  in the      micropores  on surfaces of Fe/1.2Mg Si were
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           physiological environment .                         discernible due to the relatively large amounts of
                                    [38]
             The XRD patterns of Fe/Mg Si composites are       Mg Si.
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           given in Figure 3B. It could be found from the      3.3 Mechanical properties
           figure that the detectable phase was α-Fe for all
           the  Fe/Mg Si composites,  which  was similar  to   Functionally speaking, the compression strength
                     2
           that of Fe powder in Figure 1E. Moreover, there     of bone implants was thought to be an important
           were no obvious changes in the peak positions and   indicator  since  bones need  to  be  strong enough
           relative intensities. The Mg Si peaks could not be   to survive normal activities . In this study, the
                                                                                          [42]
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           found for all the samples, which attributed to the   compression strength of Fe/Mg Si composites is
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           low contents. The metallographic micrographs of     depicted in Figure 4A. It could be found that the
           Fe/Mg Si composites are presented in Figure 3C.     compression strength gradually decreased (230 ±
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           It was seen that Fe/0.3Mg Si exhibited flexuous     15, 202 ± 20, 172 ± 12, 130 ± 10, and 88 ± 6 MPa
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           grain boundaries with grain sizes ranging from 5    for  Fe,  Fe/0.3Mg Si,  Fe/0.6Mg Si,  Fe/0.9Mg Si,
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           to 45 μm (average grain size of 29.8 ± 2.1 μm). The   and Fe/1.2Mg Si, respectively).  The  decreased
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           Fe/0.6Mg Si consisted of grain sizes ranging from   compression strength could be attributed  to the
                    2
           5 to 35 μm and its average grain size was 23.7 ±    distributions and amounts of Mg Si, which may
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           1.5 μm. The grains of Fe/0.9Mg Si were obviously    cause defects in the microstructure, as evidenced
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                                       International Journal of Bioprinting (2020)–Volume 6, Issue 1        79
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