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Compression Failure of Trabecular Tantalum Scaffolds
           the  elastic  moduli  of  AM-fabricated  trabecular  Ta   deformation and fractures appeared on the outside of the
           scaffolds with porosities of 65%, 75%, and 85% were 3.0   AM-fabricated  trabecular  Ta  scaffolds  with  porosities
           ± 0.2, 2.2 ± 0.3, and 1.1 ± 0.1 GPa, respectively, and their   of 65%, 75%, and 85% under compressive loads. Most
           yield strengths were 35.7 ± 0.8 (σ ), 19.5 ± 0.6 (σ ), and   microcracks  occurred  at  conjunctions,  and  the  rest  of
                                       y1
                                                     y2
           11.9 ± 0.5 (σ ) MPa, respectively. The yield strains of all   them  appeared  on the  struts. The  fractured  struts were
                     y3
           tested samples lie in the range between 1% and 2%.  twisted greatly. Figure 11 displays the SEM micrographs
                                                               of the ductile  fracture surface of  AM-fabricated  Ta
           3.3. Material failure study                         sample after tensile fracture failure. The interior collapse
           Figure  8 illustrates the geometrical  morphologies of   characterizations of AM-fabricated trabecular Ta scaffolds
           trabecular Ta scaffolds with porosities of 65%, 75%, and   with porosities of 65%, 75%, and 85% under compressive
           85% under compressive strains of 0, 20%, and 50%. They   loading are shown in Figures 12-14, respectively. Optical
           demonstrated  ductile  deformation  during  compression   microscope (OM) photographs indicate that both the strut
           tests, and no macroscopic cracks were found with a strain   distribution  on the  polished  cross-section  of annealed
           up to 50%. Figure 9 shows the stress–strain curve and   and unannealed specimens that underwent compression
           failed specimen of trabecular Ti6Al4V scaffold obtained   are consistent with the uncompressed specimen (control
           from the previous study .  An obvious shear fracture   group),  which  facilitates  the  identification  of  collapse
                                [36]
           band  along  the  inclination  of  45°  with  respect  to  the   characterizations of trabecular Ta scaffolds. In comparison
           loading direction was found on the trabecular Ti6Al4V   with the  control  group, only part  of the  struts inside
           scaffold. SEM micrographs (Figure 10) suggest that strut   porous  Ta  scaffolds  deformed  plastically  or  fractured

           Table 2. Compressive mechanical properties of AM-fabricated trabecular Ta scaffolds and human cancellous bone
           Testing specimen             Porosity (%)        Yield strength (MPa)        Elastic modulus (GPa)
           Ta scaffolds                      65                  35.7±0.8                      3.0±0.2
                                             75                  19.5±0.6                      2.2±0.3
                                             85                  11.9±0.5                      1.1±0.1
           Human cancellous bone           50 – 90               6.6 – 36.2                 0.88 – 3.4 [2,31-35]





































           Figure 8. Geometric morphologies of trabecular Ta scaffolds with porosities of 65%, 75%, and 85% under strains of 0, 20%, and 50%,
           respectively.

           118                         International Journal of Bioprinting (2022)–Volume 8, Issue 1
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