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Materials Science in Additive Manufacturing                       Powder alteration caused by L-PBF process


























            Figure 19. Particle-size distribution of lattices parts with different cell   Figure 21. D-values of new powder versus powder reused 12 times.
            sizes (fourth replicate for each cell size).























                                                               Figure 22. Particle-size distribution of new powder versus powder reused
            Figure 20. D-values of lattices depending on cell sizes.  12 times.

            values of powder reused 12  times. Significant increases   ratio of printed components in these lattice cylinders
            could  be  observed  in  D90,  D50,  and  D10,  of  21.7%,   changes the PSD of the powder trapped in the lattice
            16.6%, and 15.5%, respectively. The PSD moved larger   structure. This outcome might be caused by a variety of
            particles rightward, followed by a slight drop in fine   circumstances. The balling defect might be responsible
            particles and a relevant increase in the proportion of large   for the increase in powder diameter to 500  µm due to
            particles (Figure  22). This result has also been reported   the creation of partially melted particles . Furthermore,
                                                                                                [5]
            by many researchers studying the effects of reuse cycles   formation of spatters could be the primary reason for the
            on powder size characteristics [10,11,25,34,36,38-41] . For example,   increase in PSD. Soundarapandiyan et al. [11,42]  and Sutton
            Soundarapandiyan et al.  and Richard and O’Leary et al.    et  al.  observed that powder near the melt pool was
                                                        [22]
                               [11]
                                                                   [10]
            observed the same behavior of the Ti-6Al-4V powder PSD,
            which shifted rightward after five reuse cycles. In another   coarser due to the presence of spatters, partially melted
            study, we confirmed the similar PSD behavior after reusing   particles, hard sintering, and agglomerations.
            maraging steel powder 8 times .                      A small proportion of large particles in the diameter
                                    [36]
              Figure 20 shows that D-values D10 and D50 increased   range of 200–1000 µm (Figures 5, 8, 12, 14, and 22) were
            by 16.2% and 9%, respectively, while the D90 decreased by   likely aggregates in the PSDs samples analyzed by the
            13% when the area ratio was increased from 2.4 to 8.4. As a   Mastersizer 3000, since particles in this size range were not
            result, we can deduce that increasing the area and volume   observed using the electron microscope.


            Volume 2 Issue 3 (2023)                         10                      https://doi.org/10.36922/msam.1781
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