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Materials Science in Additive Manufacturing                            NiTi lattice: Performance optimization



            alloys can safely prevent excessive swaying of the piers, as   structure is less conducive to additive manufacturing. In
            demonstrated by Fang et al. who introduced NiTi washer   contrast, an emerging bionic structure, that is, the TPMS
            springs into seismic bridge design.  To explore its use in   structure, not only reduces the stress concentration at
                                        4
            orthopedic applications, Xie  et al. treated the surface of   the node but also changes the geometric characteristics
            NiTi alloy to improve surface hardness and antibacterial   of the lattice structure, making its surface smoother
            properties. 5                                      and the stress distribution more uniform. 21-23  In this
                                                               study, the body-centered cubic (BCC) lattice structure
              The NiTi porous structure features high specific
            strength  and  stiffness,  as  well  as  remarkable  mechanical   and the I-graph-wrapped package (I-WP) lattice structure
                                                               generated through minimal surface optimization were
            properties in low-density structures. The internal structure   investigated. 24,25  The I-WP curved surface, commonly
            of conventionally made NiTi porous structure is composed   referred to as I-WP, is a kind of TPMSs. The “I” denotes
            of randomly distributed pores with different shapes, giving   the BCC lattice. The “WP” is the abbreviation for “wrapped
            a random microstructure that leads to local performance   package,”  named  for  the  resemblance  of  finite  portions
            differences and affects the structure’s applications.   of the I-WP surface to string arrangement on a simply
            However, the development of additive manufacturing   wrapped package. 26
            technology has enabled the precise fabrication of NiTi
            porous structures with regular shapes inside.  Laser   Therefore, BCC and I-WP structures were selected for
                                                   6,7
            powder bed fusion (LPBF) technology is an emerging   experiments to study the forming quality and properties of
            polymer and metal additive manufacturing technology   NiTi lattice structures prepared by LPBF. The applicability
            that uses a laser or electron beam as the energy source   of the TPMS optimization design method in the field of
            to melt or sinter powder materials in a layer-by-layer   metal materials prepared by the LPBF process was also
            fashion. 8-11  Hussain et al. utilized LPBF to prepare a NiTi   investigated in this study.
            triply periodic minimal surface (TPMS) lattice, revealing   2. Methods
            the effects of process parameters and structural topology
            on microstructure characteristics. 12              2.1. Design and manufacture of lattice structures
              The service life of NiTi materials is extremely critical   2.1.1. Design of BCC and I-WP
            in applications such as cardiovascular stents  and   As shown in Figure 1, the volume fraction of the sample is
                                                     13
                        14
            helical springs.  Over the past few decades, many cyclic   10%. The unit cell is a cube with a side length of 5 mm. The
            compression experiments have been conducted on NiTi   whole sample is composed of unit cells and is a cube with a
            alloys.  Kan  et al. studied the functional degradation   side length of 20 mm.
                 15
            of superelastic NiTi  rods in cyclic tension-unloading
            and compression-unloading experiments,  while Safdel   The BCC lattice structure was designed by the 3D
                                              16
            et al. investigated the tensile-compression asymmetric   geometric modeling software Creo (Pro/E), whereas the
            behavior of NiTi alloys by laser powder bed melting.    I-WP lattice structure was parameterized using MATLAB,
                                                         17
            However, studies on the fatigue properties of NiTi alloys   and their implicit function control equations are as follows:
            remain scarce.  The experiments of Zhang et al. showed
                        18
                                                                                      
                                                                             
            that rock-like splitting and chipping through nucleation   Fx yz t(, ,, ) = 2 ( cos 2π x   cos 2π y  
                                                                             
                                                                                      
            and slow,  stable  growth  of compression-parallel cracks           L      L 
            driven by very small stress intensity are the major factors     y     z z     z     x 
                                                                   
                                                                                      
                                                                            
                                                                                              
            driving fatigue failure of the material.  Zhao and Kang   + cos 2π  L   cos 2π L   + cos 2π L   cos 2π L   )  t −  (I)
                                           19
                                                                                      
                                                                            
                                                                                              
                                                                   
            showed that the fatigue life of NiTi alloy microtubules
            would be affected by the loading path and stress level   Where L denotes the unit cell size, which was 5 mm
            under uniaxial cyclic loading.  Most of the previous   in this study, and t denotes the control volume fraction,
                                      20
            studies focused on the fatigue performance of the alloy   which was 10%.
            or the structure itself. However, there was no comparison
            between structural optimization design and fatigue   2.1.2. Materials and equipment
            performance.                                       NiTi alloy powder with an elemental ratio of 1:1 was
              For the most commonly used strut-based lattice   prepared by electrode induction melting gas atomization
            structure, the sharp pillar at the node can lead to   and  purchased  from  Avimetal  Powder  Metallurgy
            higher stress concentration, which adversely affects   Technology Co., Ltd. The density of the powder was
                                                                       3
            the mechanical properties and fatigue properties of the   6.45 g/cm . The BLT-S210 (Xi’an Bright Laser Technologies,
            sample. Furthermore, the cantilever of strut-based lattice   Ltd., China) was utilized to conduct the LPBF process.
            Volume 3 Issue 2 (2024)                         2                              doi: 10.36922/msam.3380
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