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Materials Science in Additive Manufacturing                          Gradient porous material design criteria



            struts  become stuck by  other struts,  causing  a localized   to less than one will also prevent cracks from penetrating
            reduction in porosity and resulting in densification of the   the sample without reaching any of the tougher porous
            porous material, which shows the deformation-induced   structures. Figure 6 shows the SS curves of Gyroid-sheet and
            densification phenomenon. As a result, the stress increases   Diamond-sheet gradient porosity materials with different
            with decreasing porosity until the toughness becomes too   porosity changes, and the sample is designed and divided
            high, and thus, the crack continues to propagate until it   into upper and lower layers with different porosities,
            penetrates the sample and reaches the outer surface, causing   while the 3/3 means that the upper and lower layers are
            sample failure. A similar phenomenon can be observed in   composed  of  three  layers  of  unit  cells.  In  Figure  5A,
            Figure 5, where deformation-induced densification occurs   the Gyroid-sheet uniform porosity materials with 70%
            only in porous materials with high porosity because the   porosity show less tendency of deformation-induced
            toughness at the first stress drop decreases with increasing   densification phenomenon. However, the tendency of
            porosity, as shown in Table 1. Therefore, it is expected that   deformation-induced densification phenomenon increases
            the material’s nature, lattice structure design, porosity, and   with increased porosity changes, as shown in Figure 6A.
            sample design would influence such phenomenon.     Moreover, the stress in the plateau and densification stage
                                                               increases with increased porosity changes as well. It is
              Hence, this phenomenon can be triggered artificially   because the maximum stress decreases with increased
            by introducing a tougher porous structure near the region   porosity, as shown in  Figure 7, and thus, the maximum
            where  the  struts  may  fracture.  Moreover,  limiting  the   stress of the layer with higher porosity will not exceed the
            aspect ratio of the region where the struts  may fracture   yield stress of the layer with lower porosity. This means that
                                                               when the layer with higher porosity reaches its maximum
                                                               stress, the layer with lower porosity is still in a state of
                                                               elastic deformation. Hence, only the struts in the layer with
                                                               higher-porosity fracture, and these struts are subsequently
                                                               stuck by the struts in the layer with lower porosity.
                                                                 To quantify the minimum difference between the
                                                               yield stress of the lower porosity layer and the maximum
                                                               stress of the higher porosity layer, the results in Figure 6
                                                               are crucial. As shown in  Figure  6B, the Diamond-sheet
                                                               samples with 70 – 71% porosity change was a failure
                                                               after the first stress drop, which means the slight stress
                                                               difference cannot activate the deformation-induced
                                                               densification process. However, as the porosity change
                                                               increases, the stress in the plateau stage increases, which
                                                               means that the tendency of densification also increases.
                                                               For the Diamond-sheet samples with 70 – 75% porosity,
            Figure  4. Schematic diagram of three deformation stages for uniform   the maximum stress in the plateau stage is almost the same
            porosity materials                                 as that before the first stress drop. However, for the Gyroid-

                        A                                    B


















            Figure 5. Stress-strain curves of Schon-Gyroid-sheet uniform porosity materials (A) and Schwarz-Diamond-sheet uniform porosity materials (B)

            Volume 3 Issue 3 (2024)                         5                              doi: 10.36922/msam.4234
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