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International Journal of Bioprinting                    b-Ti21S TPMS FGPs produced by laser powder bed fusion



            Table 8. Summary of Young’s modulus obtained by means of   cell size on the normal plane in the case of homogenization
            homogenization method on the single unit cell for both TPMS   analysis, a fully solid FEA of the complete specimen
            structures (nTopology software).                   with 4.0 mm and 2.5 mm unit cell size were performed,

             TPMS-FGPSs  Relative density ρ r  E  hom  (GPa)  E hom  (GPa)  as shown in  Figures 17 and  18, respectively. Thanks to
                         (−)             nom       real        Equation XII, an elastic modulus of 7.7 GPa and of 3.2 GPa
             2.5 mm      0.17            1.15     0.93         was obtained in the case of TPMS-FGPS 4.0 and TPMS-
                         0.34            4.88     4.16         FGPS 2.5, respectively. The stiffness obtained in case of
                                                               TPMS-FGPS 4 is closer to the experimental value (−25%),
                         0.50            10.83    9.77         confirming that the non-negligible edge effects occur in the
                         0.66            19.47    18.00        case of a small number of unit cells in the normal area with
                         0.83            32.5     31.13        respect to the load [64,69,70] . A similar variation with respect
             4.0 mm      0.17            1.12     0.86         to experimental results was achieved with TPMS-FGPS 2.5
                         0.34            4.88     2.79         (−27%). The deviation of approximately 25% between the
                         0.50            10.84    8.92         experimental and predicted elastic modulus through FEA
                                                               may be attributed to the fact that compression testing is not
                         0.66            19.47    16.73        an ideal quasi-static process, even at low strain rates. As
                         0.83            32.7     28.67        noted by Yang et al. , the ideal quasi-static compression
                                                                               [71]
                                                               test occurs primarily in the first layers near the applied
                                                               load, where the stress is not transmitted to lower parts.
                                                               The solid FEA analysis presented here was conducted to
            Table 9. Elastic modulus of the two TPMS-FGPSs obtained   highlight the limitations of the homogenization method
            by experimental analysis and through homogenization using   when the minimum required number of unit cell sizes
            nominal and real ligament dimensions one.          was not used. Further considerations, deriving from more

             TPMS-FGPSs  E  cyclic  (GPa)  E nom  E  hom       detailed FEA modeling, will be the subject of future works.
                                     hom
                                                real
                                    (GPa)      (GPa)           Taken together, the measurement of the Gibson–Ashby
             2.5 mm     4.1 ± 0.1   4.6 (10%)  3.8 (−8%)       constants was carried out in the case of TPMS-FGPS 2.5
                                                               since it was characterized by enough unit cell number
             4.0 mm     10.7 ± 0.1  4.2 (−61%)  3.1 (−70%)     to avoid the edge effects (Figure 19). The plot permits to
































            Figure 17. Finite element simulation of the complete TPMS-FGPS 4.0. (a) The contour mesh of the as-manufactured samples. (b) Loading condition
            resembling the experimental condition, i.e., a fixed constraint on the bottom surface of the specimen and a fixed displacement equal to 0.1 mm in the
            vertical direction on the top surface. (c) Results of the simulation analysis.


            Volume 9 Issue 4 (2023)                        203                          https://doi.org/10.18063/ijb.729
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