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Materials Science in

                                                                  Additive Manufacturing



                                        ORIGINAL RESEARCH ARTICLE
                                        The effect of thermal rest time during in situ

                                        alloying of Ti41Nb through laser powder bed
                                        fusion



                                        Guo Ren Chou , Sheng Huang 1,2  , and Swee Leong Sing *
                                                    1
                                                                                         3
                                        1 School of Mechanical and Aerospace Engineering, Nanyang Technological University, 50 Nanyang
                                        Avenue, 639798, Singapore
                                        2 Singapore Centre for 3D Printing, Nanyang Technological University, 50 Nanyang Avenue, 639798,
                                        Singapore
                                        3 Department of Mechanical Engineering, National University of University, 9 Engineering Drive 1,
                                        117575, Singapore




                                        Abstract

                                        This study investigates the impact of thermal rest time variation on in situ alloying
                                        of Ti41Nb (wt.%) within a single part, building on previous research that utilized a
                                        short stripe width scanning strategy to promote interaction between individual melt
                                        pools. Employing a contour scan from the part center outwards, diverse thermal rest
                                        times were achieved at different locations within the component. Results revealed
                                        a significant influence of varying thermal rest times on the amount of unmelted Nb
                                        and mechanical properties of the part. The findings underscore the importance of
                                        considering thermal rest time in in situ alloying and laser powder bed fusion (LPBF)
                                        printing in general, as it can markedly affect print quality. This study contributes
                                        valuable insights for optimizing LPBF processing parameters and advancing the
            *Corresponding author:
            Swee Leong Sing             understanding of in situ alloying through LPBF.
            (sweeleong.sing@nus.edu.sg)
            Citation: Chou GR, Huang S,   Keywords: Additive manufacturing; 3D Printing; Ti–Nb; Powder bed fusion; Selective
            Sing  SW. The effect of thermal rest
            time during in situ alloying of Ti41Nb   laser melting
            via laser powder bed fusion. Mater
            Sci Add Manuf. 2024;3(3):3506
            doi: 10.36922/msam.3506
            Received: April 25, 2024    1. Introduction
            Accepted: August 26, 2024   Three-dimensional (3D) printing, also known as additive manufacturing (AM),
            Published Online: September 11, 2024  constitutes one of the three fundamental automated processes, alongside subtractive and
                                        formative fabrication methods.  Unlike subtractive manufacturing, AM encompasses a
                                                                 1
            Copyright: © 2024 Author(s).
            This is an Open-Access article   range of processes that build parts based on 3D digital data, typically through layer-
            distributed under the terms of the   wise material deposition. While AM is often associated with fused deposition modeling
            Creative Commons Attribution
            License, permitting distribution,   technology, due to its commercialization and affordability for hobbyists, noteworthy
            and reproduction in any medium,   instances of AM trace back to 1987 with the launch of 3D Systems’ first commercial AM
            provided the original work is
            properly cited.             system in the US, the stereolithography apparatus-1. Since then, new AM technologies
                                        have rapidly emerged to address evolving application demands.
            Publisher’s Note: AccScience
            Publishing remains neutral with   In recent decades, metal AM has enjoyed significant advancements, owing to
            regard to jurisdictional claims in
            published maps and institutional   the development of precise high-energy sources and computational technology.
            affiliations.               This bottom-up approach allows the parts manufacturing industry to overcome


            Volume 3 Issue 3 (2024)                         1                              doi: 10.36922/msam.3506
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