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Materials Science in Additive Manufacturing                  Additive manufacturing of NASA HR-1 angled walls




                           A                       B                      C












            Figure 9. Samples were printed at (A) 0°, (B) 20°, and (C) 30° deposition angles. Scale bar: 200 µm; magnification: ×100
             A
                                B









            Figure  10. Distribution of carbides. (A) Sample 0° 1,070W shows the
            distribution of carbides within the γ matrix and (B) γ’ precipitates found in
            literature.  Red arrows indicate γ’ precipitates under optical microscope.
                  1
            Yellow arrows also indicate γ’ under scanning electron microscope. Scale
            bar: (A) 20 µm, (B) 100 µm; magnification: ×500


                                                               Figure 12. Tensile properties of laser powder direct energy deposition
                                                               heat-treated samples printed with different deposition angles deposition
                                                               or laser power
                                                               Table 5. Comparison of grain size measured on XY plane on
                                                               laser powder direct energy deposition NASA HR‑1 angled
                                                               walls
                                                               Sample                        Average grain size (µm)
                                                               0° 1,070 W                           189
                                                               0° 2,620 W                           182
                                                               20° 1,070 W                          195
                                                               20° 2,620 W                          194
            Figure  11.  Graphical comparison of microhardness on laser powder   30° 1,070 W        188
            direct energy deposition heat-treated samples deposited with different   30° 2,620 W    193
            deposition angles or laser power.
                                                               those of the other samples. This consistency can be linked
            of defects present in the 2,620 W samples did not affect   to the similar grain size across all samples. In addition,
            the ductility of the material.  However, the 20° 2,620 W   the strength shown by the alloy is likely related to the γ’
                                   28
            sample showed a slightly lower elongation of approximately   strengthening mechanism  used for this material, which
            30%. This sample also showed a significantly higher   enhances strength without compromising ductility. 1,2
            standard deviation compared to the rest, which may be
            attributed to possible local process instabilities or material   Overall, no significant differences were found when
            abnormalities, such as residual porosity, thermal stress, or   varying laser power or deposition angles, as confirmed
            internal defects.  Despite these variations, the UTS and   by the t-test. The only property that showed a statistically
                         29
            YS of sample 2,620 were not statistically different from   significant difference was the YS of the 20° 2,620 W sample


            Volume 4 Issue 1 (2025)                         7                              doi: 10.36922/msam.8069
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